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Basic Inorganic Chemistry Laboratory

Code: 199344
ECTS: 3.0
Lecturers in charge: izv. prof. dr. sc. Mirta Rubčić - Lectures
prof. dr. sc. Željka Soldin - Lectures
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Laboratory exercises 45
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
COURSE CONTENT: 1. Anhydrous metal halides: Preparation CuCl; 1.2. Preparation CuI; 1.3. Preparation FeCl3; 1.4. Preparation (NH4)2PbCl6 .
2. Metal acetates: 2.1. Preparation Pb(OCOCH3)4; 2.2. Preparation Zn4O(OCOCH3)6; 2.3. Preparation Cu(OCOCH3)2(H2O) 2
3. Oxides and peroxides: 3.1. Preparation Cu2O; 3.2. Preparation Cr2O3; 3.3. Preparation BaO2x8H2O
4. Double salts: 4.1. Preparation (NH4)2Mn(SO4)2x6H2O; 4.2 Preparation (NH4)2Cu(SO4)2x6H2O; 4.3. Preparation (NH4)2Ni(SO4)2x6H2O
5. Oxalate complexes - preparation and composition determination: 5.1. Preparation K3Cr(C2O4)3x3H2O; 5.2. Preparation K3Fe(C2O4)3x3H2O; 5.3. Preparation K3Al(C2O4)3x3H2O; 5.4. Preparation K2Cu(C2O4)2x2H2O
6. Complex compounds of cobalt(II) and cobalt(III); 6.1. Preparation HgCo(NCS)4 ; 6.2. Preparation Na3Co(NO2)6 ;
7. Ammine metal complexes; 7.1. Preparation Ni(NH3)6Cl2; 7.2. Preparation Co(CO3)(NH3)4NO3x0.5 H2O; 7.3. Preparation Ni(C2H8N2)3Cl2x2H2O;
8. Beta-diketone metal complexes; 8.1. Preparation Fe(C5H7O2)3; 8.2. Preparation Cu(C5H7O2)2; 8.3. Preparation Al(C5H7O2)3; 8.4. Preparation VO(C5H7O2)2
Students are obliged to make one particular preparation of each group of compounds, record IR-spectra of the one sample and perform thermogravimetric measurements -TG/DTA/DSC of the one appropriate sample .

LEARNING OUTCOMES: By the end of this course students will be able to: - use the basic methods of synthesis of inorganic compounds
- apply basic principles of chemical analysis and characterization of chemical compounds
- compare the structure of the matter and its reactivity
- demonstrate the knowledge and understanding of the basic experimental methods, instruments and way of processing the experimental dana
- set, perform and discuss the school experiments in chemistry
apply all safety precautions in handling with laboratory ware, equipment and chemicals
- perform the standard laboratory procedures
- present the results of its own research on educational and scientific meetings
- track by itself development of the new knowledge in physics and chemistry and in education of physics and chemistry
- take responsibility for its own competence advantage and professional growth
Literature:
  1. Z. Popović, Ž. Soldin, M. Đaković, Osnovni praktikum anorganske kemije, Skripta za internu upotrebu (za studente integriranog preddiplomskog i diplomskog sveučilišnog studija Biologija i kemija; smjer; nastavnički i za studente integriranog preddiplomskog i diplomskog sveučilišnog studija Fizika i kemija; smjer; nastavnički), PMF, Zagreb, 2020.
Prerequisit for:
Enrollment :
Enrolled : Inorganic Chemistry 2
Passed : Basic Laboratory in Analytical Chemistry
Attended : Inorganic Chemistry 1
6. semester
Mandatory course - Mandatory studij - Physics and Chemistry Education
Consultations schedule: