Department of...
 
Crystal Structure...
 
Crystal Structure Determination by Diffraction...
 
Code: 51066
ECTS: 4.0
Lecturers in charge: prof. dr. sc. Dubravka Matković-Čalogović - Lectures
doc. dr. sc. Ivica Đilović - Lectures
Lecturers: Ivica Đilović - Exercises
Dubravka Matković-Čalogović - Exercises
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Lectures 30
Exercises 15
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
COURSE GOALS: To learn about X-ray diffraction methods of determination of crystal and molecular structures.

LEARNING OUTCOMES AT THE LEVEL OF THE PROGRAMME:

1. KNOWLEDGE AND UNDERSTANDING
1.1. demonstrate a thorough knowledge and understanding of the fundamental laws of classical and modern physics
1.2. demonstrate a thorough knowledge and understanding of the most important chemistry laws and theories
2. APPLYING KNOWLEDGE AND UNDERSTANDING
2.2. describe important aspects of chemical change
2.9. use information and communication technology efficiently (to foster active enquiry, collaboration and interaction in the classroom);
5. LEARNING SKILLS
5.1. search for and use professional literature as well as any other sources of relevant information

LEARNING OUTCOMES SPECIFIC FOR THE COURSE:
1. Understanding advantage/dissadvantage of X-ray structure analysis for specific samples in comparison to other diffraction methods (neutron and electron diffraction).
2. Describing sources and detectors of X-rays, neutrons and electrons.
3. Usage of the basic concepts of symmetry, crystal lattice, diffraction and intesities of diffracted maxima.
4. Describing the problem of phases.
5. Collection of diffraction data, solving and refining crystal structures and their graphical presentation by using the appropriate programs.
6. Searching crystallographic databases.

COURSE DESCRIPTION:
x -ray sources, crystals, crystallization techniques, diffraction theory, experimental methods, phase problem, Fourier transformations, structure refinement, geometry analysis and presentation of solved structures.

REQUIREMENTS FOR STUDENTS:
To follow the lectures, to pass 2 colloquia, to accomplish 1 seminar

GRADING AND ASSESSING THE WORK OF STUDENTS:
A grade structure: the colloquia, seminars and written examination.
Literature:
  1. 1. C. Giacovazzo et al.: Fundamentals of Crystallography, 2. izdanje, Oxford Univ. Press, Oxford 2002.
  2. 2. Jan Drenth: Principles of Protein Crystallography, 3. izdanje, Springer Science, 2007.
  3. 3. I. Vicković: Difrakcijske metode određivanja kristalnih struktura, interna skripta, 1996.
Prerequisit for:
Enrollment :
Passed : Fundamentals of Physics 4
Passed : Mathematics 4
Attended : Physical Chemistry
7. semester
Izborni - kemija 3 - Mandatory studij - Physics and Chemistry Education

8. semester
Izborni - kemija 3 - Mandatory studij - Physics and Chemistry Education
Consultations schedule:
News
 
No news!
Repository
 
Repository is empty
Poll
 
No polls currently selected on this page!

 

 

Sva prava pridržana. Kemijski odsjek Prirodoslovno-matematičkog fakulteta
Sveučilište u Zagrebu