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Chromatographic Methods in Analytics

Code: 152861
ECTS: 8.0
Lecturers in charge: doc. dr. sc. Mario Cindrić - Lectures
prof. dr. sc. Vlasta Drevenkar - Lectures
prof. dr. sc. Nives Galić - Lectures
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Lectures 20
Seminar 10
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
The types of chromatography analytical techniques: relative to aggregate states of stationary and mobile phase, performance, and physicochemical processes. Theory of chromatographic processes. Factors that influence chromatographic processes. Separation efficiency and selectivity. Generating of chromatographic analytical data and data processing. Analyte characterization and quantitative analysis of specific mixture components. Selection of chromatographic method relative to analyte chemical properties. Sample preparation prior to chromatographic analysis.
Liquid Chromatography (LC): Stationary and mobile phase properties. Adequate instrumental and detection techniques for specific analyte analysis. High Performance Liquid Chromatography: liquid adsorption chromatography, partition liquid chromatography. Normal- and reversed-phase chromatography. Ion-pair chromatography. Chiral chromatography. Ion-exchange chromatography. Size exclusion chromatography. Multidimensional chromatography and hyphenated instrumental techniques. Chromatographic separation and protein mixture analysis. Applications.
Gas Chromatography (GC): Selection of suitable mobile and stationary phases. Gas-liquid chromatography. Adsorption chromatography. Design of gas chromatography system. Multidimensional chromatography and hyphenated instrumental techniques. Applications.
Supercritical fluid chromatography. Properties of mobile and stationary phases. Design of chromatography system.
Capillary electrophoresis. Principle. Adequate instrumental and detection techniques. Capillary electrochromatography. Micellar electrokinetic chromatography. Applications.
description of instruction methods Lectures, seminars, laboratory demonstrations, consultations
description of course/module requirements Written and oral exam
Literature:
  1. OBVEZNA LITERATURA:
    P. Worsfold, A. Townshend, C. Poole (ur.): Encyclopedia of Analytical Science, Second Edition, Elsevier Ltd., Oxford 2005.
    M. Kaštelan-Macan, M. Medić-Šarić, S. Turina: Plošna kromatografija, Farmaceutsko-biokemijski fakultet Sveučilšta u Zagrebu, Zagreb 2006.
    I. Piljac: Elektroforeza, Media Print, Zagreb 2006.
    R. E. Ardrey: Liquid Chromatography-mass spectrometry: An introduction, John Wiley & Sons Ltd., Chichester 2005.
    M. Kaštelan-Macan, M. Petrović (ur.):Analitika okoliša, Hinus&Fakultet kemijskog inženjerstva i tehnologije Sveučilišta u Zagrebu, Zagreb, 2013.
    L. T. Taylor, Supercritical Fluid Chromatography, Anal. Chem. 82 (2010)4925-4935.
    J. V. Seeley, S. K. Seeley, Multidimensional Gas Chromatography: Fundamental Advances and New Applications, Ana.l Chem. 85 (2013)557-578.
  2. DOPUNSKA LITERATURA:
    Suvremeni opsežniji revijski članci i znanstvene monografije
1. semester
Temeljni kolegiji iz analitičke kemije - Mandatory smjer - Analytical chemistry
Izborni kolegiji za smjer biokemija - Mandatory smjer - Biochemistry
Izborni kolegiji za smjer anorganska i strukturna kemija - Mandatory smjer - Inorganic and structural chemistry
Izborni kolegiji za smjer organska kemija - Mandatory smjer - Organic chemistry
Izborni kolegiji za smjer fizikalna kemija - Mandatory smjer - Physical chemistry

3. semester
Izborni predmeti doktorski studij kemije - Mandatory smjer - Analytical chemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Biochemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Inorganic and structural chemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Organic chemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Physical chemistry
Consultations schedule: