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Spectroscopic structural analysis

Code: 44004
ECTS: 5.0
Lecturers in charge: prof. dr. sc. Predrag Novak - Lectures
Lecturers: Tomislav Jednačak - Seminar
Ivana Mikulandra - Seminar
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Lectures 30
Seminar 15
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
Electromagnetic radiation. Electromagnetic spectrum. Interactions between electromagnetic radiation and matter. Absorption, emission, scatering. Basic principles of NMR, IR and UV spectroscopy and mass spectrometry. Structural parameters and isomery. Functional groups and their spectral properties. One- and two-dimensional NMR techniques and spectral interpretation. IR and Raman spectra - group vibrations. Mass spectra - fragmentation and ions. UV spectra -chomophores. Ways of solving structural problems. Understanding the ways of interpreting spectra. Steps in establishing a molecular structure. Combination of NMR, IR, MS and UV data in an interactive manner. Molecular formula, functional groups, substructures, working structures. Identification, 2D structure, conformation, configuration. Principles in determining 3D molecular structure by combining NMR and molecular modeling methods.
EXPECTED COMPETENCES TO BE ACQUIRED:
- to understand and explain concepts of spectroscopic structural analysis
- do develop skills and competences for solving molecular structure
- to understand ways of interpreting spectra
- to compare advantages and disadvantages of spectroscopic methods for structure determination
- to choose the most appropriate approach to solve 2D and 3D molecular structure
- to apply gained knowledge and skills in scientific research
- to develop team work skills
Literature:
  1. P. Novak i T. Jednačak, Strukturna analiza spojeva spektroskopskim metodama, TIVA Tiskara, Varaždin, 2013.
  2. R. M. Silverstein, F. X. Webster, D. J. Kiemle Spectrometric Identification of Organic Compounds, John Wiley & Sons, New York, 2005.
  3. E. Pretch, P. Bühlmann i C. Affolter: Structure Determination of Organic Compounds-Tables of spectral data, Springer, Berlin, 2009.
  4. L.D.Field, S. Sternhell, J.R. Kalman, Organic Structures from Spectra, Wiley, Chichester, 2004.
  5. T. D. W. Claridge, High Resolution NMR Techniques in Organic Chemistry, Pergamon, Amsterdam, 2009.
  6. E. de Hoffman, V. Stroobant, Mass Spectrometry-Principles and Applications, Wiley, Chichester, 2003
    scientific papers
Prerequisit for:
Enrollment :
Attended : Multidimensional NMR spectroscopy
2. semester
Izborni predmeti analitička kemija - Mandatory smjer - Analytical and inorganic chemistry
Izborni predmeti analitička kemija - Mandatory smjer - Analytical and organic chemistry
Izborni predmeti analitička kemija - Mandatory smjer - Analytical and physical chemistry
Izborni predmeti analitička kemija - Mandatory smjer - Analytical chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Physical and organic chemistry

4. semester
Izborni predmeti analitička kemija - Mandatory smjer - Analytical and inorganic chemistry
Izborni predmeti analitička kemija - Mandatory smjer - Analytical and organic chemistry
Izborni predmeti analitička kemija - Mandatory smjer - Analytical and physical chemistry
Izborni predmeti analitička kemija - Mandatory smjer - Analytical chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Physical and organic chemistry
Consultations schedule: