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Advanced organic laboratory course
 
Code: 44053
ECTS: 5.0
Lecturers in charge: izv. prof. dr. sc. Vesna Petrović Peroković - Lectures
doc. dr. sc. Ivana Biljan - Lectures
Lecturers: Željka Car - Practicum
Zoran Glasovac - Practicum
Ivan Kodrin - Practicum
Đani Škalamera - Practicum
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Practicum 60
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
COURSE CONTENT:
Research database search and literature citing; Mannich reaction; Oxidative phenolic coupling; Quaternary ammonium salts; Chemical resolution of enantiomers and chiral HPLC analysis; Perkin condensation; Knoevenagel reaction (microwave synthesis) ; Enantioselective reduction (biocatalysis; polarimetry); Molecular modelling.

LEARNING OUTCOMES:
After completion of this course, the successful student will be able to:
- use laboratory dishes, to prepare the apparatus and to carry out classical and advanced organic laboratory procedures
- use high performance liquid chromatography ( HPLC ) for analysis of the mixture and determining the optical purity
- identify the reaction products on the basis of IR and NMR spectra
- specify and to explain the modern organic synthetic methods
- perform conformational analysis by applying computational chemistry
- plan a multistep synthesis of organic compounds
- use scientific and professional literature and other relevant sources of information.
Literature:
  1. 1. Interna skripta
    2. A. I. Vogel: A Text-book of Practical Organic Chemistry, 5. izdanje, Longman, London, 1989.
    3. R. M. Silverstein, G. C. Bassler, T. C. Morrill, Spectrometric Identification of Organic Compounds, 5. izdanje, John Wiley & Sons, New York, 1991.
  2. J. Clayden, N. Greeves, S. Warren and P. Wothers, Organic Chemistry, Oxford Press, 2001.
  3. J. A. Moore, D. L. Dalrymple, Experimental Methods in Organic Chemistry, W.B. Saunders Comp., 1976.
  4. S. H. Pine, Organska kemija, Školska knjiga, Zagreb, 1994.
  5. J. March, Advanced Organic Chemistry, John Wiley & Sons, New York, 2001.
  6. J. Mann, R. S. Davidson, J. B. Hobbs, D. V. Banthorpe and J. B. Harborne, Natural Products, Longman Ltd., UK, 1994.
  7. A. R. Leach, Molecular Modelling, Principles and Applications, 2nd Ed., Longman, 2001.
  8. C. J. Cramer, Essentials of Computational Chemistry, Wiley, 2002.
1. semester
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and inorganic chemistry
Mandatory course - Mandatory smjer - Analytical and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical chemistry and biochemistry
Mandatory course - Mandatory smjer - Biochemistry and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Mandatory course - Mandatory smjer - Inorganic and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic chemistry and biochemistry
Mandatory course - Mandatory smjer - Physical and organic chemistry

3. semester
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and inorganic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic chemistry and biochemistry
Consultations schedule:
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