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Instrumental analysis 1

Code: 43971
ECTS: 5.0
Lecturers in charge: izv. prof. dr. sc. Sanda Rončević - Lectures
Lecturers: Ivan Nemet - Seminar
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Lectures 30
Seminar 15
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
COURSE CONTENT
Spectrometric methods of analysis, optical spectrometer construction, interferometers, excitation sources, detectors; Basic features of atomic spectrometry instruments, flame and electrothermic atomic absorption, flame photometry, plasma optical and mass spectrometry, electric arc and spark, glow discharge spectrometry, atomic and X-ray flourescence; Basic features of molecular spectrometry instruments, UV/VIS spectrophotometry, vibration spectrocopy in infrared, Raman spectroscopy, luminescence techniques. Electroanalytical methods (potentiometry,voltammetry,culometry). Instrument performances for specific analytical claims; Development and applications of specialized instrumental techniques (laser ablation, hydride generation, flow injection analyis, cold vapour techniques, automatization).
LEARNING OUTCOMES
1. To describe basic components of optical spectrometers
2. To explain principal characteristics of radiation source in optical instruments
3. To compare properties and functions of photon and thermic detectors
4. To classify instrumental methods according to interaction of radiation and matter
5. To describe analytical characteristics of emission methods (flame photometry, plasma spectrometry, glow discharge)
6. To describe analytical characteristics of atomic absorption spectrometry (flame, electrothermic)
7. To explain principal characteristics of instruments in quantitative molecular spectrometry (UV/VIS spectrophotometer, fluorimeter)
8. To explain fundamental properties of dispersive and non-dispersive instruments in vibration spectroscopy (IR, Raman)
9. To compare advantages and disadvantages of particular analytical instruments in sample characterization
10. To predict the selection of instrumental method in special analytical claims (analysis of content, reactivity and structure)
Literature:
  1. 1. D. A. Skoog, F. J. Holler, S. R. Crouch, Principles of Instrumental Analysis, 6th Ed., Thomson Brooks/Cole, Belmont, USA, 2007.
  2. 1. S. J. Hill, Inductively Coupled Plasma Spectrometry and its Applications, Blackwell Publishing Ltd. Oxford, 2007.
    2. A. Sanz-Medel, R. Pereiro, Atomic Absorption spectrometry: An Introduction, 2nd Ed., Momentum Press, 2014.
    3. J. D. Ingle, S.R. Crouch, Spectrochemical Analys, Prentice-Hall International Inc, Englewood Cliffs, 1988.
    4. R. Kellner et al., Analytical Chemistr, Wiley-VCH, Wienheim, 1998.
1. semester
Mandatory course - Mandatory smjer - Analytical and inorganic chemistry
Mandatory course - Mandatory smjer - Analytical and organic chemistry
Mandatory course - Mandatory smjer - Analytical and physical chemistry
Mandatory course - Mandatory smjer - Analytical chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Physical and organic chemistry

3. semester
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Inorganic chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Physical and organic chemistry
Consultations schedule: