Phase and elemental analyis

Phase and elemental analyis

Code: 44125
ECTS: 5.0
Lecturers in charge: prof. dr. sc. Darko Tibljaš - Lectures
izv. prof. dr. sc. Gordana Medunić - Lectures
Take exam: Studomat
English level:

1,0,0

All teaching activities will be held in Croatian. However, foreign students in mixed groups will have the opportunity to attend additional office hours with the lecturer and teaching assistants in English to help master the course materials. Additionally, the lecturer will refer foreign students to the corresponding literature in English, as well as give them the possibility of taking the associated exams in English.
Load:

1. komponenta

Lecture typeTotal
Lectures 15
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
Qualitative and quantitative parameters of the analytical method choice. Sampling plan design and selection of the best posible methods. Preselection of the analytical samples, methods of sample dissolution and destruction. Stoihiometric calculations in the wet chemistry methods. Absorption and emission spectrometric methods, instrumental optical components. Mass spectrometry methods, Moessbauer spectroscopy, nuclear activation analytical methods. Mineral separation methods. X-ray powder diffraction (factors influencing diffracted beam intensity, unit cell dimensions calculation from powder patterns, powder pattern fitting techniques). X-ray fluorescence analysis (matrix problem and methods for solving it, sample preparation). Electron microscopy (SEM, EBSD, chemical analyisis, electron diffraction).

Learning outcomes:

Knowledge and understanding of the scientific and technical terminology in the domain of analytical chemistry.
Ability to understand specific aspects of analytical methods in chemistry (the problem of analytical precision, significant digits, figures of merit).
Ability to analyse the results of chemical analysis by statistical means.
Capability of performing classical silicate analysis.
Knowledge and understanding of factors influencing the measured parameters on X-ray powder pattern and related ability to overcome possible problems.
Literature:
  1. Jones, M.P. (1997): Methoden der Mineralogie. Ferdinand Enke Verlag, Stuttgart, 260 str
  2. Skoog, D.A. & Leary, J.J. (1992): Principles of instrumental analysis. Saunders College Publishing, Fort Worth, 700 str.
  3. Skoog, D.A., West, D.M. & Holler, F.J. (1999): Osnove analitičke kemije. Školska knjiga, Zagreb, 951 str.
  4. Whiston, C. (1987): X-ray metods, John Wiley & Sons, New York, 426 str.
1. semester
Izborni kolegiji za smjer Mineralogija i petrologija (zimski semestar) - Mandatory studij - Graduate Study of Geology

3. semester
Izborni kolegiji za smjer Mineralogija i petrologija (zimski semestar) - Mandatory studij - Graduate Study of Geology
Consultations schedule:

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