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Analytical chemistry 2
 
Code: 41010
ECTS: 5.0
Lecturers in charge: prof. dr. sc. Predrag Novak - Lectures
Lecturers: Tomislav Jednačak - Seminar
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Lectures 45
Seminar 30
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
Analytics; analytical process; analytical signal; classical and instrumental analytical methods; electromagnetic spectrum; interaction of electromagnetic radiation and matter; Absorption, emission, scattering; Atomic spectra ? electron transitions in atoms and ions; Emission, absorption and fluorescence spectroscopy; Molecular spectra; Spectral line intensity; Dependence of intensity on concentration; Absorption of ultraviolet and visible light as analytical information; Lambert-Beer law; Functional groups as chromophores and ausochromes; Luminescence analysis; Fluorescence, phosphorescence; chemiluminescence; Infrared spectra (IR); Selection rules; Group vibrations; Vibrational coupling; Fingerprint region; Raman spectra (Ra); Selection rules; Complementarity with IR; Nuclear magnetic resonance spectroscopy (NMR); spin and resonance, vector model; radiofrequency pulse, NMR parameters - relaxation, chemical shift (nuclear shielding), couplings; spin systems; one- and two-dimenzional NMR techniques; spectra interpretation, Solid state NMR spectroscopy; Mass spectrometry - ionisation and, molecular ion; mass analyzers, fragmentation and mass spectrum; introduction to spectroscopic structure
COURSE CONTENT:
Analytical signal; Interaction of radiation with atoms and molecules; Absorption, emission, scattering, basic theory of atomic and molecular spectroscopy; Selection rules; Electronic spectra and their features (functional groups and their effects on spectra); Fluorimetry and other lliminescences; Infrared spectra and group vibrations: Raman spectroscopy- Complementary to infrared; Magnetic resonance; NMR and EPR spectra; Chemical shifts and coupling constants; 1D and 2D spectra; Mass cpectrometry-ionization, Desorpling and frangmentation; Basic chromatography; Other metods (survey).
Literature:
  1. D. A. Skoog, D. M. West, F. J. Holler: Osnove analitičke kemije, prijevod: N. Kujundžić, V. Allegretti Živčić, A. Živković, Školska knjiga, Zagreb 1999
  2. D. A. Skoog, J. F. Holler, S. R. Crouch, Principles of Instrumental Analysis, 6. izd., Thomson, Belmont, 2007.
  3. H. Naumer i W. Heller (ur.): Untersuchungsmethoden in der Chemie, Georg Thieme, Stuttgart 3. izd., Wiley-VCH, Weinheim, 2002.
  4. D. A. Skoog, D. M. West, F. J. Holler, S. R. Crouch : Fundamentals of Analytical Chemistry, 8. izd., Thomson, 2004.
  5. P. Novak. T. Jednačak, Strukturna analiza spojeva spektroskopskim metodama, TIVA Tiskara, Varaždin, 2013.
  6. H. Günzler, I. H.-U. Gremlich: Uvod u infracrvenu spektroskopiju, prijevod: Z. Meić, G. Baranović, Školska knjiga, Zagreb 2006.
  7. H. Fribolin: Basic One- and Two-dimensional NMR Spectroscopy, 4. izd., VCH, Weinheim 2005.
  8. E. de Hoffmann, V. Stroobant: Mass Spectrometry, 2. izd., Wiley, Chichester 2002.
Prerequisit for:
Examination :
Passed : Analytical chemistry 1
4. semester
Mandatory course - Mandatory studij - Chemistry
Consultations schedule:
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