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Diffraction methods of crystal structure...
 
Code: 43978
ECTS: 5.0
Lecturers in charge: prof. dr. sc. Dubravka Matković-Čalogović - Lectures
doc. dr. sc. Ivica Đilović - Lectures
Lecturers: Ivica Đilović - Seminar
Dubravka Matković-Čalogović - Seminar
Take exam: Studomat
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1. komponenta

Lecture typeTotal
Lectures 30
Seminar 15
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
COURSE CONTENT:
X-ray sources, basics of symmetry, crystal lattice, crystallization techniques, diffraction and intensity of diffraction maxima. Comparison of different experimental methods used in structure solving procedures. Phase problem, the role of Fourier transforms and convolution in structure solving, structure refinement, geometry analysis and presentation of solved crystal and molecular structures.

LEARNING OUTCOMES:
1. Explaining advantage/disadvantage of X-ray structure analysis for specific samples in comparison to other diffraction methods (neutron and electron diffraction).
2. Describing sources and detectors of X-rays, neutrons and electrons.
3. Usage of the basic concepts of symmetry, crystal lattice, diffraction and intesities of diffracted maxima.
4. Describing the problem of phases.
5. Collection of diffraction data, solving and refining crystal structures and their graphical presentation by using the appropriate programs.
6. Searching crystallographic databases
Literature:
  1. 1. C. Giacovazzo et al.: Fundamentals of Crystallography, 2. izdanje, Oxford Univ. Press, Oxford 2002.
  2. 2. Jan Drenth: Principles of Protein Crystallography, 3. izdanje, Springer Science, 2007.
  3. 3. I. Vicković: Difrakcijske metode određivanja kristalnih struktura, interna skripta, 1996.
2. semester
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Analytical and inorganic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Inorganic and organic chemistry
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Inorganic chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Physical and organic chemistry

4. semester
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Analytical and inorganic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical and physical chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Analytical chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and organic chemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Biochemistry and physical chemistry
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Inorganic and organic chemistry
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Inorganic and physical chemistry
Izborni predmeti anorganska i strukturna kemija - Mandatory smjer - Inorganic chemistry and biochemistry
Izborni predmeti izvan odabranih grana - Mandatory smjer - Physical and organic chemistry
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