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Atomic Spectrometry in Analytics
 
Code: 152859
ECTS: 8.0
Lecturers in charge: izv. prof. dr. sc. Sanda Rončević - Lectures
Take exam: Studomat
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1. komponenta

Lecture typeTotal
Lectures 20
Seminar 10
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
Atomic spectrometry methods in analysis of elements, historical development, present state, application to individual elements. Preparation of samples: sampling, storage, mineralization, extraction and concentration of elements before analysis. Sources of contamination. Theory of atomic spectrometry: absorption, emission and fluorescence.
Atomic absorption spectrometry (AAS): basic principle (instrumentation, techniques, automation, sources of energy), calibration, atomization in flame, electrothermal atomization, interference effects, background correction, special techniques (cold vapor, hydride generation).
Atomic emission spectrometry (AES): flame, plasma, glow discharge as excitation sources; spectrometer constructions; detection of emission signal. Advanced instrumental techniques based on hyphenated systems: gas and liquid chromatography, capillary electrophoresis, glow discharges coupled with plasma and/or mass spectrometer. Comparison of methods: detection limits, concentration range, efficiency in analytical demands.
Environmental risk assessment (chemical species and adaptation, estimation of bioavailability, variations, representative species and deficiency, extrapolation laboratory-enviro152859nment); analytical monitoring of environmental impacts; modern instrumental methods in quality control; essential and toxic materials, additives; present scope and challenges in forming of new regulative procedures
description of instruction methods Lectures, seminars, laboratory demonstrations, consultations
description of course/module requirements Written and/or oral exam
Literature:
  1. OBVEZNA LITERATURA:
    S. J. Hill, Inductively Coupled Plasma Spectrometry and its Applications, Blackwell Publishing Ltd. Oxford, 2007.
    A. Sanz-Medel, R. Pereiro, Atomic Absorption spectrometry: An Introduction, 2nd Ed., Momentum Press, 2014.
    J.A.C. Broekaert, Analytical Atomic Spectrometry with Flames and Plasmas, Wiley-VCH, Wieinheim, 2001.
    D. A. Skoog, F. J. Holler, S. R. Crouch, Principles of Instrumental Analysis, 6th Ed., Thomson Brooks/Cole, Belmont, USA, 2007.
    J. Noelte, ICP Emission Spectrometry - A Practical Guide, Wiley-VCH, Weinheim, 2003.
    R. Cornelis, Handbook of Elemental Speciation - Techniques and Methodology, J. Wiley & Sons Ltd, The Atrium, Southern Gate, Chichester, England, 2003.
    J. D. Ingle, S.R. Crouch, Spectrochemical Analys, Prentice-Hall International Inc, Englewood Cliffs, 1988.
  2. DOPUNSKA LITERATURA:
    Suvremeni opsežniji revijski članci i znanstvene monografije
1. semester
Temeljni kolegiji iz analitičke kemije - Mandatory smjer - Analytical chemistry
Izborni kolegiji za smjer biokemija - Mandatory smjer - Biochemistry
Izborni kolegiji za smjer anorganska i strukturna kemija - Mandatory smjer - Inorganic and structural chemistry
Izborni kolegiji za smjer organska kemija - Mandatory smjer - Organic chemistry
Izborni kolegiji za smjer fizikalna kemija - Mandatory smjer - Physical chemistry

3. semester
Izborni predmeti doktorski studij kemije - Mandatory smjer - Analytical chemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Biochemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Inorganic and structural chemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Organic chemistry
Izborni predmeti doktorski studij kemije - Mandatory smjer - Physical chemistry
Consultations schedule:
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