Department of...
 
Inorganic...
 
Inorganic Chemistry Laboratory
 
Code: 46843
ECTS: 2.0
Lecturers in charge: izv. prof. dr. sc. Mirta Rubčić - Lectures
prof. dr. sc. Željka Soldin - Lectures
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Practicum 30
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
1. ANHYDROUS METAL HALIDES
1.1. Preparation of copper(I) chloride
1.2. Preparation of copper(I) iodide
1.3. Preparation of iron(III) chloride
1.4. Preparation of ammonium hexachloroplumbate(IV)
2. METAL ACETATES
2.1. Preparation of plumbum(IV) acetate
2.2. Priprava of basic zinc(II) acetate
2.3. Preparation diaquatetrakis(mu-acetate)dicopper(II)
3. OXALATE METAL COMPLEXES
3.1. Preparation of potassium tris(oxalate)chromate(III) trihydrate
3.1.1. Determination of the complex composition
3.2. Preparation of potassium tris(oxalate)ferate(III) trihydrate
3.2.1. Determination of the complex composition
3.3. Preparation of potassium tris(oxalate)aluminate(III) trihydrate
3.3.1. Determination of the complex composition
3.4. Preparation of potassium diaquabis(oxalate)cuprate(II)
3.4.1. Determination of the complex composition
4. COMPLEXES OF COBALT(II) AND COBALT(III)
4.1. Preparation of mercury(II) tetra(thiocyanate-N)cobaltate(II)
4.2. Preparation of sodium hexanitrocobaltate(III)
5. METAL COMPLEXES WITH NITROGEN LIGANDS
5.1. Preparation of hexaamminenickel(II) chloride
5.2. Preparation of tetraamminecarbonatecobalt(II) nitrate hemihydrates
5.3. Preparation of tris(ethylenedimaine)nickel(II) chloride dehydrate
6. 2,4-PENTANEDIONATO METAL COMPLEXES
6.1. Preparation of tris(pentane-2,4-dionate)iron(III)
6.2. Preparation of bis(pentane-2,4-dionate)copper(II)
6.3. Preparation of tris(pentane-2,4-dionate)aluminium(III)
6.4. Preparation of bis(pentane-2,4-dionate)oxovanadium(IV)
7. RECORDING AND CHARACTERIZATION OF IR-SPECTRA IN SOLID STATE (two samples)

Expected competences to be acquire:

Student will know:
- the basic methods of synthesis of inorganic compounds
- principles of chemical analysis and characterization of chemical compounds
Student will be able:
- to compare the structure of the matter and its reactivity
- to demonstrate the knowledge and understanding of the basic experimental methods, instruments and way of processing the experimental data
- set, perform and discuss the school experiments in chemistry
- to apply all safety precautions in handling with laboratory ware, equipment and chemicals
- perform the standard laboratory procedures
- to introduce the results of its own research on educational and scientific meetings
- to track by itself development of the new knowledge in physics and chemistry and in education of physics and chemistry
Student will be able to take responsibility for its own competence advantage and professional growth.
Literature:
  1. Z. Popović, Ž. Soldin, M. Đaković, Praktikum iz anorganske kemije-upute za internu uporabu, Kemijski odsjek, Prirodoslovno-matematički fakultet, Zagreb, 2017.
5. semester
Mandatory course - Mandatory studij - Biology and Chemistry Education
Consultations schedule:
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Sva prava pridržana. Kemijski odsjek Prirodoslovno-matematičkog fakulteta
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