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Higher laboratory in chemistry

Code: 72853
ECTS: 5.0
Lecturers in charge: doc. dr. sc. Ivana Kekez
Lecturers: prof. dr. sc. Tajana Begović - Laboratory exercises
dr. sc. Mladen Borovina - Laboratory exercises
izv. prof. dr. sc. Nikola Bregović - Laboratory exercises
Petra Kozulić , mag. chem. - Laboratory exercises
doc. dr. sc. Ivan Nemet - Laboratory exercises
Barbara Panić , mag. chem. - Laboratory exercises
prof. dr. sc. Biserka Prugovečki - Laboratory exercises
Gregor Talajić , mag. chem. - Laboratory exercises
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Laboratory exercises 60
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
1. SOLVOTHERMAL AND MECHANOCHEMICAL SYNTHESIS
1.1. Preparation of azidepicolinamidocopper(II), in solution and by mechanochemical pathway
1.2. Preparation of bis(picolinamidato)copper(II) dihydrate, , solvothermally
2. PREPARATION OF TARGETED ORGANIC LIGANDS
2.1. Prepartion of trans-cinnamon acid
2.2. Preparation of acetylsalicyl acid
2.3. Preparation of N-benzoyl glycine
I. Preparation of calcium complex with N-benzoyl glycine
II. Preparation of zinc complex with N-benzoyl glycine
III. Preparation of vanadium(IV) complex with N-benzoyl glycine
IV. Preparation of aqua(1,10-phenantroline-N,N')(malonate-O,O')copper(II) monohydrate,
3. EXTRACTION AND DETERMINATION OF POLYPHENOL CONTENT IN THE REAL SAMPLE BY HPLC TECHNIQUE
4. ATOMIC EMISSION SPECTROSCOPY WITH INDUCTIVELY COUPLED PLASMA
5. METAL COMPLEXES BIOLOGICAL ACTIVITY INVESTIGATION
6. DISSOCIATION EQUILIBRIUM OF WEAK ACID
7. EXPERIMENTAL DETERMINATION OF EQUILIBRIUM DISSOCIATION CONSTANT OF CINNAMON ACID
8. FINAL EXERCISE
Literature:
1. semester
Mandatory course - Regular study - Chemistry Education
Consultations schedule: