1. komponenta

Lecture type	Total
Laboratory exercises	60

* Load is given in academic hour (1 academic hour = 45 minutes)

1. SOLVOTHERMAL AND MECHANOCHEMICAL SYNTHESIS
1.1. Preparation of azidepicolinamidocopper(II), in solution and by mechanochemical pathway
1.2. Preparation of bis(picolinamidato)copper(II) dihydrate, , solvothermally
2. PREPARATION OF TARGETED ORGANIC LIGANDS
2.1. Prepartion of trans-cinnamon acid
2.2. Preparation of acetylsalicyl acid
2.3. Preparation of N-benzoyl glycine
I. Preparation of calcium complex with N-benzoyl glycine
II. Preparation of zinc complex with N-benzoyl glycine
III. Preparation of vanadium(IV) complex with N-benzoyl glycine
IV. Preparation of aqua(1,10-phenantroline-N,N')(malonate-O,O')copper(II) monohydrate,
3. EXTRACTION AND DETERMINATION OF POLYPHENOL CONTENT IN THE REAL SAMPLE BY HPLC TECHNIQUE
4. ATOMIC EMISSION SPECTROSCOPY WITH INDUCTIVELY COUPLED PLASMA
5. METAL COMPLEXES BIOLOGICAL ACTIVITY INVESTIGATION
6. DISSOCIATION EQUILIBRIUM OF WEAK ACID
7. EXPERIMENTAL DETERMINATION OF EQUILIBRIUM DISSOCIATION CONSTANT OF CINNAMON ACID
8. FINAL EXERCISE

1. Viši praktikum kemije, Skripta za internu upotrebu, Z. Popović, I. Juranović Cindrić, R. Ribić, J. Rokov-Plavec, T. Preočanin, N. Bregović,, PMF, Zagreb, 2004.
2. Experimental Inorganic Chemistry, W. G. Palmer, Cambridge University Press, 1954.
3. Practical Inorganic Chemistry, G. Marr, B. W. Rockett, Van Nostrand Reinhold Company, London, 1972.
4. Synthesis and Technique in Inorganic Chemistry, 3rd Ed., G. S. Girolami, T. B. Rauchfuss, R. J. Angelici, University Science Books, Sausalito, CA, 1999.
5. Inorganic Experiments, D. J. Woollins, VCH, Weinheim, 1994.
6. Mikrobiolooške metode za određivanje antibiotičke aktivnosti, u Metode u molekularnoj biologiji ur. A. Ambriović Ristov, J. Šušković, B. Kos, Institut Ruđer Bošković, 2007.
7. Physical Chemistry, 8th Ed., P. Atkins, J. de Paula, Oxford University Press, Oxford, 2007.
8. A Text-book of Practical Organic Chemistry, 5th. Ed., A. I. Vogel, Longman, London, 1989.
9. Inorganic Laboratory Preparations, G. G. Schlessinger, Chemical Publishing Company, Inc., New York, 1962.

Mandatory course - Regular study - Chemistry Education