1. komponenta

Lecture type	Total
Laboratory exercises	60

* Load is given in academic hour (1 academic hour = 45 minutes)

1. SOLVOTHERMAL AND MECHANOCHEMICAL SYNTHESIS
1.1. Preparation of azidepicolinamidocopper(II), in solution and by mechanochemical pathway
1.2. Preparation of bis(picolinamidato)copper(II) dihydrate, , solvothermally
2. PREPARATION OF TARGETED ORGANIC LIGANDS
2.1. Prepartion of trans-cinnamon acid
2.2. Preparation of acetylsalicyl acid
2.3. Preparation of N-benzoyl glycine
I. Preparation of calcium complex with N-benzoyl glycine
II. Preparation of zinc complex with N-benzoyl glycine
III. Preparation of vanadium(IV) complex with N-benzoyl glycine
IV. Preparation of aqua(1,10-phenantroline-N,N')(malonate-O,O')copper(II) monohydrate,
3. EXTRACTION AND DETERMINATION OF POLYPHENOL CONTENT IN THE REAL SAMPLE BY HPLC TECHNIQUE
4. ATOMIC EMISSION SPECTROSCOPY WITH INDUCTIVELY COUPLED PLASMA
5. METAL COMPLEXES BIOLOGICAL ACTIVITY INVESTIGATION
6. DISSOCIATION EQUILIBRIUM OF WEAK ACID
7. EXPERIMENTAL DETERMINATION OF EQUILIBRIUM DISSOCIATION CONSTANT OF CINNAMON ACID
8. FINAL EXERCISE

1. Z. Popović, I. Juranović Cindrić, R. Ribić, J. Rokov-Plavec, T. Preočanin, N. Bregović,: Viši praktikum kemije, Skripta za internu upotrebu
2. W. G. Palmer: Experimental Inorganic Chemistry
3. G. Marr, B. W. Rockett: Practical Inorganic Chemistry
4. G. S. Girolami, T. B. Rauchfuss, R. J. Angelici: Synthesis and Technique in Inorganic Chemistry, 3rd Ed.
5. D. J. Woollins: Inorganic Experiments
6. J. Šušković, B. Kos: Mikrobiolooške metode za određivanje antibiotičke aktivnosti, u Metode u molekularnoj biologiji ur. A. Ambriović Ristov
7. P. Atkins, J. de Paula: Physical Chemistry, 8th Ed.
8. A. I. Vogel: A Text-book of Practical Organic Chemistry, 5th. Ed.
9. G. G. Schlessinger: Inorganic Laboratory Preparations

Mandatory course - Regular study - Chemistry Education