Advanced Chemistry Laboratory

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Advanced Chemistry Laboratory

Code: 208617
ECTS: 4.0
Lecturers in charge: doc. dr. sc. Ivana Kekez
Lecturers: prof. dr. sc. Tajana Begović - Practicum
dr. sc. Mladen Borovina - Practicum
izv. prof. dr. sc. Nikola Bregović - Practicum
dr. sc. Iva Habinovec - Practicum
Petra Kozulić , mag. chem. - Practicum
doc. dr. sc. Ivan Nemet - Practicum
Barbara Panić , mag. chem. - Practicum
Gregor Talajić , mag. chem. - Practicum
Take exam: Studomat
Load:

1. komponenta

Lecture typeTotal
Practicum 60
* Load is given in academic hour (1 academic hour = 45 minutes)
Description:
1. SOLVOTHERMAL AND MECHANOCHEMICAL SYNTHESIS
1.1. Preparation of azidepicolinamidocopper(II), in solution and by mechanochemical pathway
1.2. Preparation of bis(picolinamidato)copper(II) dihydrate, , solvothermally

2. PREPARATION OF TARGETED ORGANIC LIGANDS
2.1. Prepartion of trans-cinnamon acid
2.2. Preparation of acetylsalicyl acid
2.3. Preparation of N-benzoyl glycine
I. Preparation of calcium complex with N-benzoyl glycine
II. Preparation of zinc complex with N-benzoyl glycine
III. Preparation of vanadium(IV) complex with N-benzoyl glycine
IV. Preparation of aqua(1,10-phenantroline-N,N')(malonate-O,O')copper(II) monohydrate,

3. EXTRACTION AND DETERMINATION OF POLYPHENOL CONTENT IN THE REAL SAMPLE BY HPLC TECHNIQUE

4. ATOMIC EMISSION SPECTROSCOPY WITH INDUCTIVELY COUPLED PLASMA

5. METAL COMPLEXES BIOLOGICAL ACTIVITY INVESTIGATION

6. DISSOCIATION EQUILIBRIUM OF WEAK ACID

7. EXPERIMENTAL DETERMINATION OF EQUILIBRIUM DISSOCIATION CONSTANT OF CINNAMON ACID

8. FINAL EXERCISE
Literature:
Prerequisit for:
Enrollment :
Passed : Algae and Fungi
Passed : Analytical Chemistry 2
Passed : Basic Biochemistry Laboratory
Passed : Basic Inorganic Chemistry Laboratory
Passed : Basic Laboratory in Physical Chemistry
Passed : Basic Organic Chemistry Laboratory
Passed : Fundamentals of Evolution
Passed : Fundamentals of Microbiology
Passed : Organic Chemistry 2
Passed : Pedagogy
Passed : Physical Chemistry 2
7. semester
Mandatory course - Regular study - Biology and Chemistry Education
Consultations schedule: